..,1 ..2
1 ,
, .
2.
2 , , . 3.
: ..
, , , [1]. , , . [2].
γ- . 4--3-( -)- [3].
.
( ) - , .
, .
POLPHARMA SA (10 ), , , - .
Agilent Technologies 6890N (USA) - EVDX-5MS, 0,2 × 25 × 0,33 .
LC-20 Prominence (Shimadzu, Japan) - (120×5 , 14 , 2,5 /) -2 (200×6 , 100-200 , 12 /).
-- 100 /. . 2,0 /. , m/z 138, 103, 237.
, , , : 4-( -)--2- 4-( -)--2-. 50 /.
|
|
, (>10) (=9,6) [4].
4--3-( -)- . , 120 /, 30 /.
4-( -)--2- - . : m/z 138, 103, 237.
. 30 /.
:
[1] , .., .. - .: -, 2000, 204 .
[2] .., .., .., .., .., .. . - 51, 2326 (2008)
[3] , .. . M.: , 1995, 562 .
[4] European Pharmacopoeia 6th Edition, Supplement 6.1. Strasbourg: European Directorate for the Quality of Medicines, 2007, 310 p.